Chemistry 232, Quantitative Analysis


Professor Robert G. Michel (Lecture Instructor)
Dr. Larry Springsteen (Laboratory Instructor)
Department of Chemistry
University of Connecticut

The Laboratory Manual

Outline (reading and writing assignments marking scheme, etc)

The Experiments

Instructions for use of the Analytical Balance GA7 Potentiometric acid-base titration
Practice Sheet for Analytical Balance expt. GA8 Ion selective electrode determination of fluoride in toothpaste, mouthwash, etc.
GA1 Mass and Volume GA10 Determination of water in acetonitrile by Gas Chromatography
GA2 KHP Analysis GA12 Spectrophotometric determination of phenacitin and caffeine in coffee and tea
The following two experiments are done with pairs of students:
GA3 Ca by Homogeneous Precipitation
GA4 Ca by EDTA titration
GA16 Interference effects and characteristics of the determination of calcium by atomic absorption spectrophotometry
GA5 Iodimetric Titration of Vitamin C tablets GA20 High Performance Liquid Chromatographic Separation Of Various Compounds Found In Soda, Coffee And Tea
GA6 iron in ore by potassium dichromate titr. GA21 Spectrophotometric Determination of iron

How to use a laboratory notebook correctly

The format for laboratory reports

Statistical Tables ("F", "Q" and "t" tests)

Checkout Procedures

Academic Misconduct

In many of your lab. reports, and some of your homeworks and examinations, you will be allowed to work with another student in order to develop your assigned work. This is in the spirit of scientific collaboration. However, you are not allowed to hand in the same document as your partner, neither are parts of a docment allowed to be the same between two students. Only jointely collected data can be the same. If you work jointly, then you should write up the work separately. Further, when you write documents you are expected to use many different textbooks and journals, but you are not allowed to plagarise words or figures from such sources. Use your own words, and draw simplified versions of the figures for your reports. You are not allowed to change numbers in your laboratory notebook at any time. Any alterations will be assumed to be "fudged" data, and appropriate penalties will be imposed.

Plagarism and illigitimate alterations to scientific data are classed as serious academic misconduct. An important part of the University's guidelines on academic misconduct is reproduced here as a reminder: